2020Theoretical Foundations of Chemical EngineeringRequires access

Synthesis of Boehmite Nanosized Powder (AlOOH) at Low Temperatures of Hydrothermal Treatment

И. В. Козерожец, G. P. Panasyuk, Е. А. Семенов, Н. П. Симоненко, Л. А. Азарова, В. Н. Белан

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Abstract

Abstract A method is proposed for the synthesis of nanoscale boehmite powder at low temperatures of hydrothermal treatment in 1.5 wt % HCl solution at 150 and 170°C and in water at 80, 100, and 130°C. The optimal parameters of hydrothermal treatment are found. The conversion stages of γ-Al2O3 to boehmite (AlOOH) are found; the process is solid-phase (topochemical). The physical and technological properties of boehmite nanopowder are studied. We have found that boehmite possesses similar properties despite the temperature of hydrothermal treatment.

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Abstract A method is proposed for the synthesis of nanoscale boehmite powder at low temperatures of hydrothermal treatment in 1.5 wt % HCl solution at 150 and 170°C and in water at 80, 100, and 130°C. The optimal parameters of hydrothermal treatment are found. The conversion stages of γ-Al2O3 to boehmite (AlOOH) are found; the process is solid-phase (topochemical). The physical and technological properties of boehmite nanopowder are studied. We have found that boehmite possesses similar properties despite the temperature of hydrothermal treatment.

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Available abstract

Abstract A method is proposed for the synthesis of nanoscale boehmite powder at low temperatures of hydrothermal treatment in 1.5 wt % HCl solution at 150 and 170°C and in water at 80, 100, and 130°C. The optimal parameters of hydrothermal treatment are found. The conversion stages of γ-Al2O3 to boehmite (AlOOH) are found; the process is solid-phase (topochemical). The physical and technological properties of boehmite nanopowder are studied. We have found that boehmite possesses similar properties despite the temperature of hydrothermal treatment.

Key concepts: Boehmite, Hydrothermal circulation, Materials science, Chemical engineering, Hydrothermal synthesis, Phase (matter), Chemistry, Metallurgy

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