2020Journal of Nanoscience and NanotechnologyRequires access

Rapid Synthesis of Uniform CdSe Nanorods by a Microwave-Assisted Solvothermal Method in Ethylenediamine

Maokun Han, Ruijuan Qi

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Abstract

A rapid microwave-assisted solvothermal method is reported for the synthesis of uniform CdSe nanorods in ethylenediamine (EDA) using CdCl₂ and elemental Se as reactants. The resultant nanorods have a diameter of approximately 10 nm and a length of approximately 300 nm. Our experiments show that the concentrations of EDA and CdCl₂ play important roles in product morphology. The well-dispersed CdSe nanorods with high aspect ratios were characterized by X-ray diffraction (XRD), transmission electron microscopy (TEM), energy-dispersive X-ray (EDX), UV-vis absorption and photoluminescence (PL).

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What this paper is about

A rapid microwave-assisted solvothermal method is reported for the synthesis of uniform CdSe nanorods in ethylenediamine (EDA) using CdCl₂ and elemental Se as reactants. The resultant nanorods have a diameter of approximately 10 nm and a length of approximately 300 nm. Our experiments show that the concentrations of EDA and CdCl₂ play important roles in product morphology. The well-dispersed CdSe nanorods with high aspect ratios were characterized by X-ray diffraction (XRD), transmission electron microscopy (TEM), energy-dispersive X-ray (EDX), UV-vis absorption and photoluminescence (PL).

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Available abstract

A rapid microwave-assisted solvothermal method is reported for the synthesis of uniform CdSe nanorods in ethylenediamine (EDA) using CdCl₂ and elemental Se as reactants. The resultant nanorods have a diameter of approximately 10 nm and a length of approximately 300 nm. Our experiments show that the concentrations of EDA and CdCl₂ play important roles in product morphology. The well-dispersed CdSe nanorods with high aspect ratios were characterized by X-ray diffraction (XRD), transmission electron microscopy (TEM), energy-dispersive X-ray (EDX), UV-vis absorption and photoluminescence (PL).

Key concepts: Nanorod, Ethylenediamine, Materials science, Photoluminescence, Transmission electron microscopy, Absorption (acoustics), Chemical engineering, Solvothermal synthesis

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