1969Journal of AOAC INTERNATIONALRequires access

TLC Determination of Uncombined 2-Naphthol-6-Sulfonic Acid (Sodium Salt) (Schaeffer Salt) in Color Additives

Lueangier Moten, CHRISTINE M. KOTTEMANN

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Abstract

Abstract A thin layer chromatographic method is presented for determining uncombined sodium salt of 2-naphtliol-6-sulfonic acid (Schaeffer salt) in Ext. D&C Green No. 1. A direct fluorometric measurement may also be used to determine Schaeffer salt in Ext. D&C Green No. 1 and in FD&C Yellow No. 6. Uncombined Schaeffer salt in commercial samples of FD&C Yellow No. 6 varied from 0 to 0.5%; no samples of External D&C Green No. 1 were found to contain >0.1% of uncombined Schaeffer salt.

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Abstract A thin layer chromatographic method is presented for determining uncombined sodium salt of 2-naphtliol-6-sulfonic acid (Schaeffer salt) in Ext. D&C Green No. 1. A direct fluorometric measurement may also be used to determine Schaeffer salt in Ext. D&C Green No. 1 and in FD&C Yellow No. 6. Uncombined Schaeffer salt in commercial samples of FD&C Yellow No. 6 varied from 0 to 0.5%; no samples of External D&C Green No. 1 were found to contain >0.1% of uncombined Schaeffer salt.

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Available abstract

Abstract A thin layer chromatographic method is presented for determining uncombined sodium salt of 2-naphtliol-6-sulfonic acid (Schaeffer salt) in Ext. D&C Green No. 1. A direct fluorometric measurement may also be used to determine Schaeffer salt in Ext. D&C Green No. 1 and in FD&C Yellow No. 6. Uncombined Schaeffer salt in commercial samples of FD&C Yellow No. 6 varied from 0 to 0.5%; no samples of External D&C Green No. 1 were found to contain >0.1% of uncombined Schaeffer salt.

Key concepts: Salt (chemistry), Chemistry, Sodium salt, Sulfonic acid, Sodium, Nuclear chemistry, Chromatography, Inorganic chemistry

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