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1966•Journal of AOAC INTERNATIONALRequires access

Raceophenidol in Feed

Edward L. Pratt, Morris E. Auerbach

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Abstract

Abstract Raceophenidol in feed can be estimated by an ultraviolet spectrophotometric measurement of the derived p-methylsulfonylbenzaldehyde. The method, effective for measurement of raceophenidol in feed at medication levels greater than 0.002%, is based on amide hydrolysis and subsequent periodate oxidation. Collaborative studies were conducted on the method; average value was 98.5 ± 7.8%. The method is recommended for adoption as official, first action.

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What this paper is about

Abstract Raceophenidol in feed can be estimated by an ultraviolet spectrophotometric measurement of the derived p-methylsulfonylbenzaldehyde. The method, effective for measurement of raceophenidol in feed at medication levels greater than 0.002%, is based on amide hydrolysis and subsequent periodate oxidation. Collaborative studies were conducted on the method; average value was 98.5 ± 7.8%. The method is recommended for adoption as official, first action.

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Available abstract

Abstract Raceophenidol in feed can be estimated by an ultraviolet spectrophotometric measurement of the derived p-methylsulfonylbenzaldehyde. The method, effective for measurement of raceophenidol in feed at medication levels greater than 0.002%, is based on amide hydrolysis and subsequent periodate oxidation. Collaborative studies were conducted on the method; average value was 98.5 ± 7.8%. The method is recommended for adoption as official, first action.

Key concepts: Periodate, Hydrolysis, Amide, Value (mathematics), Ultraviolet, Action (physics), Chromatography, Chemistry

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