Robert F. Cunico
Abstract
Abstract The title compound (IV) is prepared from trimethylvinylsilane (I) by three different methods: Addition of nitryl chloride (II) to (I) gives the (1‐chloro‐2‐nitroethyl)silane (III) which undergoes dehydrochlorination upon heating with anhydrous sodium acetate to yield (IV).
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Abstract The title compound (IV) is prepared from trimethylvinylsilane (I) by three different methods: Addition of nitryl chloride (II) to (I) gives the (1‐chloro‐2‐nitroethyl)silane (III) which undergoes dehydrochlorination upon heating with anhydrous sodium acetate to yield (IV).
Key concepts: Chemistry, Anhydrous, Yield (engineering), Silane, Sodium, Medicinal chemistry, Chloride, Organic chemistry