2016•ChemInformRequires access

ChemInform Abstract: Structural and Vibrational Properties of Phase‐Pure Monoclinic NdLuO3 Interlanthanides Synthesized from Nanostructured Precursors.

Júlia C. Soares, Kisla P.F. Siqueira, Roberto Luiz Moreira, Anderson Dias

Abstract

Abstract Phase‐pure monoclinic NdLuO3 is prepared by hydrothermal reaction of an alkaline (pH <13) solution of Nd(NO3)3 and Lu(NO3)3 (autoclave, 250 °C, 24 h) resulting in the nanocrystalline precursors LuO(OH) and Nd(OH)3 which are further calcined, compressed, and sintered in air (1600 °C, 8 h).

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Key concepts: Monoclinic crystal system, Autoclave, Chemistry, Nanocrystalline material, Calcination, Hydrothermal reaction, Phase (matter), Hydrothermal circulation