2014•Journal of the Chinese Chemical SocietyRequires access

One‐pot Green Synthesis of Azides from Alcohols Using Brønsted Acidic Ionic Liquid [HMIM][BF 4 ] as Solvent and Catalyst

Bhaskar Garg, Yong‐Chien Ling

Abstract

Abstract Brønsted acidic ionic liquid, [HMIM][BF 4 ], has been used as a non‐volatile, eco‐friendly solvent, and catalytic medium for the one‐pot green synthesis of azides from corresponding alcohols. The [HMIM][BF 4 ] showed high reactivity than [BMIM][BF 4 ] and [BMIM][PF 6 ], affording azides in up to 97% yield, which could be easily separated from the reaction mixture. The ease of recyclability of [HMIM][BF 4 ] makes the reaction economically and potentially viable for practical applications.

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Key concepts: Chemistry, Ionic liquid, Catalysis, Yield (engineering), Solvent, Green chemistry, Organic chemistry, Reactivity (psychology)