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2018•Chemical CommunicationsRequires access

Implementing one-shot multiple-FID acquisition into homonuclear and heteronuclear NMR experiments

Kumar Motiram‐Corral, Míriam Pérez‐Trujillo, Pau Nolis, Teodor Parella

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Abstract

Multiple-FID acquisition (MFA) within the same scan is applied to acquire simultaneously multiple 2D spectra from a single NMR experiment. A discussion on the incorporation of the MFA strategy in several homonuclear and heteronuclear 2D pulse sequences is presented. As a proof of concept, a set of novel COSY, TOCSY and HMBC experiments are reported as a time-efficient solution in small-molecule NMR spectroscopy.

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What this paper is about

Multiple-FID acquisition (MFA) within the same scan is applied to acquire simultaneously multiple 2D spectra from a single NMR experiment. A discussion on the incorporation of the MFA strategy in several homonuclear and heteronuclear 2D pulse sequences is presented. As a proof of concept, a set of novel COSY, TOCSY and HMBC experiments are reported as a time-efficient solution in small-molecule NMR spectroscopy.

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OpenAlex reports 17 citations for this work. Citation counts describe recorded attention and do not establish research quality.

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Available abstract

Multiple-FID acquisition (MFA) within the same scan is applied to acquire simultaneously multiple 2D spectra from a single NMR experiment. A discussion on the incorporation of the MFA strategy in several homonuclear and heteronuclear 2D pulse sequences is presented. As a proof of concept, a set of novel COSY, TOCSY and HMBC experiments are reported as a time-efficient solution in small-molecule NMR spectroscopy.

Key concepts: Homonuclear molecule, Heteronuclear molecule, Nuclear magnetic resonance spectroscopy, Pulse sequence, Chemistry, Two-dimensional nuclear magnetic resonance spectroscopy, Nuclear magnetic resonance, Analytical Chemistry (journal)

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