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2018•ACS Sustainable Chemistry & EngineeringRequires access

Green and Direct Synthesis of Benzaldehyde and Benzyl Benzoate in One Pot

Mina Ghahremani, Rosaria Ciriminna, Valerica Pandarus, Antonino Scurria, Valeria La Parola, Francesco Giordano, Giuseppe Avellone, François Béland, Babak Karimi, Mario Pagliaro

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Abstract

High yields of valued benzaldehyde and benzyl benzoate are obtained in one pot starting from benzyl alcohol using oxygen as only oxidant under mild conditions (2 bar O 2, 100 °C) along with an ultralow amount (0.02 mol %) of Au nanoparticles heterogenized over a spherical ORMOSIL mesoporous support. The process is remarkably selective and the catalyst is stable.

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What this paper is about

High yields of valued benzaldehyde and benzyl benzoate are obtained in one pot starting from benzyl alcohol using oxygen as only oxidant under mild conditions (2 bar O 2, 100 °C) along with an ultralow amount (0.02 mol %) of Au nanoparticles heterogenized over a spherical ORMOSIL mesoporous support. The process is remarkably selective and the catalyst is stable.

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Available abstract

High yields of valued benzaldehyde and benzyl benzoate are obtained in one pot starting from benzyl alcohol using oxygen as only oxidant under mild conditions (2 bar O 2, 100 °C) along with an ultralow amount (0.02 mol %) of Au nanoparticles heterogenized over a spherical ORMOSIL mesoporous support. The process is remarkably selective and the catalyst is stable.

Key concepts: Benzaldehyde, Benzyl alcohol, Benzyl benzoate, Ormosil, Catalysis, Organic chemistry, Chemistry, Mesoporous material

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