ScholarLens Back to search
2016•Kufa Journal for ChemistryRequires access

Cloud Point Extraction Method for Separation, Extraction and Spectrophotometric Determination of Zn(II) and Ni(II) as Chloro Anion Complex by use of Crystal Violet

Jihan .R . Muslim

Open publisher page 3 citations

Abstract

Sensitive extraction method is used for separation preconcentration coupled with spectrophotometric determination of Zinc(II) and Nickel(II) as chloro anions from acidic HCl media by using crystal violet after formation ion pair association complex after studied the optimum condition for extraction demonstrated 1.5M HCl for Zn+2and 1M HCl for Ni2+, with 50 μg Zn2+ and Ni2+ , 0.7mL 1% TritonX-100 for extraction ion pair association of Zn2+ as well as 0.9mL with Ni2+ and 800C suitable for formation CPL and extraction ion pair complex for both metal ions ,with 10 minutes of heating in thermostatic water bath for Zn2+ and 15 minutes for Ni2+ then study involved effect of interferences and electrolyte with spectrophotometric determination in different samples. The wave length for maximum absorbance of ion pair complex extracted was λmax=590nm for Zn2+and 595nm for Ni2+complexes.

About this research paper

What this paper is about

Sensitive extraction method is used for separation preconcentration coupled with spectrophotometric determination of Zinc(II) and Nickel(II) as chloro anions from acidic HCl media by using crystal violet after formation ion pair association complex after studied the optimum condition for extraction demonstrated 1.5M HCl for Zn+2and 1M HCl for Ni2+, with 50 μg Zn2+ and Ni2+ , 0.7mL 1% TritonX-100 for extraction ion pair association of Zn2+ as well as 0.9mL with Ni2+ and 800C suitable for formation CPL and extraction ion pair complex for both metal ions ,with 10 minutes of heating in thermostatic water bath for Zn2+ and 15 minutes for Ni2+ then study involved effect of interferences and electrolyte with spectrophotometric determination in different samples. The wave length for maximum absorbance of ion pair complex extracted was λmax=590nm for Zn2+and 595nm for Ni2+complexes.

Why it matters

OpenAlex reports 3 citations for this work. Citation counts describe recorded attention and do not establish research quality.

Key contribution

A contribution statement is not available in the OpenAlex record.

Method / approach

Method details are not available in the OpenAlex metadata.

Main findings

Findings are not separately available in the OpenAlex metadata.

Limitations

Limitations are not available in the OpenAlex metadata.

Applications

Application details are not available in the OpenAlex metadata.

Available abstract

Sensitive extraction method is used for separation preconcentration coupled with spectrophotometric determination of Zinc(II) and Nickel(II) as chloro anions from acidic HCl media by using crystal violet after formation ion pair association complex after studied the optimum condition for extraction demonstrated 1.5M HCl for Zn+2and 1M HCl for Ni2+, with 50 μg Zn2+ and Ni2+ , 0.7mL 1% TritonX-100 for extraction ion pair association of Zn2+ as well as 0.9mL with Ni2+ and 800C suitable for formation CPL and extraction ion pair complex for both metal ions ,with 10 minutes of heating in thermostatic water bath for Zn2+ and 15 minutes for Ni2+ then study involved effect of interferences and electrolyte with spectrophotometric determination in different samples. The wave length for maximum absorbance of ion pair complex extracted was λmax=590nm for Zn2+and 595nm for Ni2+complexes.

Key concepts: Crystal violet, Extraction (chemistry), Absorbance, Zinc, Ion-association, Chemistry, Nickel, Electrolyte

Related papers

Related paper 1Related paper 2Related paper 3
Back to paper searchBrowse research topicsOriginal source
Cloud Point Extraction Method for Separation, Extraction and Spectrophotometric Determination of Zn(II) and Ni(II) as Chloro Anion Complex by use of Crystal Violet — Research Paper | ScholarLens