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2002•Chemistry LettersRequires access

Synthesis of NiS Nanowhiskers via Surfactant-aid Hydrothermal Reaction

Bo Xie, Yang Jiang, Shengwen Yuan, Qing Li, Yue Wu, Ji Wu, Yitai Qian

Open publisher page 6 citations

Abstract

Abstract Uniform NiS nanowhiskers have been prepared via a hydrothermal reaction between NiCl2•6H2O and Na2S2O3 in the presence of surfactant of C17H33COOK (potassium oleate). The images characterized through XRD and TEM indicates the morphology of hexagonal NiS is uniform nanowhiskers with an average diameter of 80 nm and length in micrometer scale. The formation mechanism and surfactant effect were discussed in details.

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What this paper is about

Abstract Uniform NiS nanowhiskers have been prepared via a hydrothermal reaction between NiCl2•6H2O and Na2S2O3 in the presence of surfactant of C17H33COOK (potassium oleate). The images characterized through XRD and TEM indicates the morphology of hexagonal NiS is uniform nanowhiskers with an average diameter of 80 nm and length in micrometer scale. The formation mechanism and surfactant effect were discussed in details.

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Available abstract

Abstract Uniform NiS nanowhiskers have been prepared via a hydrothermal reaction between NiCl2•6H2O and Na2S2O3 in the presence of surfactant of C17H33COOK (potassium oleate). The images characterized through XRD and TEM indicates the morphology of hexagonal NiS is uniform nanowhiskers with an average diameter of 80 nm and length in micrometer scale. The formation mechanism and surfactant effect were discussed in details.

Key concepts: Hydrothermal circulation, Pulmonary surfactant, Chemistry, Chemical engineering, Hexagonal crystal system, Hydrothermal synthesis, Micrometer, Nanotechnology

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