2008•Journal of Tonghua Normal UniversityRequires access

Hydrothermal Synthesis and Crystal Structure of Three-dimensional Coordination Polymer {[Co(4,4'-bipy)(H_2O)_4](4-abs)_2·2H_2O}_n

Niu Yan-ling

Abstract

A three-dimensional coordination polymer {[Co(4,4'-bipy)(H2O)4](4-abs)2·2H2O}n was synthesized by hydrothermal reaction of CoCl2·6H2O,4-Aminobenzene-sulfonate and 4,4'-Bipyridine.The structure was characterized by elemental analysis and single-crystal X-ray diffraction.It crystallizes in monoclinic crystal system,spacegroup P2(1),crystallographic data:a=11.362(9),b=8.007(6),c=15.639(12),β=92.797(11),V=1421(2)3,Z=2,Mr=687.47,Dc=1.607g/cm3,F(000)=702,μ=0.827mm-1,R1=0.0574,wR2=0.0876.

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Key concepts: Monoclinic crystal system, Crystallography, Hydrothermal circulation, Crystal structure, Coordination polymer, Hydrothermal synthesis, Chemistry, Hydrothermal reaction