Catalytic synthesis of cyclohexanone 1, 2 propanediol ketal with modified coal active carbon catalyst
Ding Shujua, Wanyi Liu
Abstract
Ding Shujua, Wanyi Liu
Abstract
The synthesis of cyclohexanone 1, 2 propanediol ketal using modified coal active carbon as the catalyst was carried out. The influences of reaction conditions were also investigated. The optimum reaction conditions were: based on 0.1 molar cyclohexanone, the molar rate of cyclohexanone to 1,2 propanediol ketal 1:1.5,the amount of catalyst 2.4% (based on the mass of total materials) ,The volume of cyclohexane was 9. 0mL, the reaction time 2h. On the conditions, the yield of the product was 85.9% and the catalyst showed high activity.
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The synthesis of cyclohexanone 1, 2 propanediol ketal using modified coal active carbon as the catalyst was carried out. The influences of reaction conditions were also investigated. The optimum reaction conditions were: based on 0.1 molar cyclohexanone, the molar rate of cyclohexanone to 1,2 propanediol ketal 1:1.5,the amount of catalyst 2.4% (based on the mass of total materials) ,The volume of cyclohexane was 9. 0mL, the reaction time 2h. On the conditions, the yield of the product was 85.9% and the catalyst showed high activity.
Key concepts: Cyclohexanone, Catalysis, Chemistry, Cyclohexane, Yield (engineering), Molar ratio, Propanediol, Organic chemistry