ScholarLens Back to search
2006•Chinese Journal of Analysis LaboratoryRequires access

Determination of phoxim residues in carrot juice concentrate by HPLC

Zhou Hong-chen

Open publisher page 0 citations

Abstract

A method for the determination of phoxim in carrot juice concentrate was established by HPLC with a DAD detector.Residues of Phoxim were extracted from samples with ethyl acetate,purified on the column of silica gel.The HPLC conditions were RP-C_(18) column,methanol-water 7∶3(V/V) as mobile phase,and wavelength at 285 nm.The linear range was 0.1～10.0 μg/mL(r=0.99985) and the regression equation was Y=48.676X-1.4548.The detection limit of Phoxim was 0.02 mg/kg in the samples of carrot and the ranges of recoveries were 76.5%～89.3%,RSD was 2.8%～4.5%.

About this research paper

What this paper is about

A method for the determination of phoxim in carrot juice concentrate was established by HPLC with a DAD detector.Residues of Phoxim were extracted from samples with ethyl acetate,purified on the column of silica gel.The HPLC conditions were RP-C_(18) column,methanol-water 7∶3(V/V) as mobile phase,and wavelength at 285 nm.The linear range was 0.1～10.0 μg/mL(r=0.99985) and the regression equation was Y=48.676X-1.4548.The detection limit of Phoxim was 0.02 mg/kg in the samples of carrot and the ranges of recoveries were 76.5%～89.3%,RSD was 2.8%～4.5%.

Why it matters

A significance statement is not available in the OpenAlex record.

Key contribution

A contribution statement is not available in the OpenAlex record.

Method / approach

Method details are not available in the OpenAlex metadata.

Main findings

Findings are not separately available in the OpenAlex metadata.

Limitations

Limitations are not available in the OpenAlex metadata.

Applications

Application details are not available in the OpenAlex metadata.

Available abstract

A method for the determination of phoxim in carrot juice concentrate was established by HPLC with a DAD detector.Residues of Phoxim were extracted from samples with ethyl acetate,purified on the column of silica gel.The HPLC conditions were RP-C_(18) column,methanol-water 7∶3(V/V) as mobile phase,and wavelength at 285 nm.The linear range was 0.1～10.0 μg/mL(r=0.99985) and the regression equation was Y=48.676X-1.4548.The detection limit of Phoxim was 0.02 mg/kg in the samples of carrot and the ranges of recoveries were 76.5%～89.3%,RSD was 2.8%～4.5%.

Key concepts: Phoxim, Chemistry, Chromatography, High-performance liquid chromatography, Detection limit, Daucus carota, Ethyl acetate, Linear relationship

Related papers

Related paper 1Related paper 2Related paper 3
Back to paper searchBrowse research topicsOriginal source
Determination of phoxim residues in carrot juice concentrate by HPLC — Research Paper | ScholarLens