Study on Rheological Properties of Mg_(0.7)Zn_(0.3)TiO_3 Slurry for Gelcasting Process
Tai Qiu
Abstract
Tai Qiu
Abstract
The M7Z3T powder was prepared by traditional solid reaction process.The effects of the addition of dispersant(PAA-NH4),pH value,solid loading of slurry,content of monomer(AM) and the ratio of monomer to coupling agent(MBAM) on rheological properties of slurries were investigated.The results showed that when pH value is 10,the dispersant content is 0.7wt%,for the 52vol% slurries,the initial viscosity is only 0.459 Pa·s.The best conditions were the amount of monomer 10wt%,the ratio of monomer to coupling agent 20∶ 1,the content of initiator 1wt% and the polymerize temperature 60 ℃.The resultant green body has uniform structure and the bending strength is as high as 24.47 MPa.
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The M7Z3T powder was prepared by traditional solid reaction process.The effects of the addition of dispersant(PAA-NH4),pH value,solid loading of slurry,content of monomer(AM) and the ratio of monomer to coupling agent(MBAM) on rheological properties of slurries were investigated.The results showed that when pH value is 10,the dispersant content is 0.7wt%,for the 52vol% slurries,the initial viscosity is only 0.459 Pa·s.The best conditions were the amount of monomer 10wt%,the ratio of monomer to coupling agent 20∶ 1,the content of initiator 1wt% and the polymerize temperature 60 ℃.The resultant green body has uniform structure and the bending strength is as high as 24.47 MPa.
Key concepts: Dispersant, Slurry, Materials science, Rheology, Monomer, Green body, Viscosity, Chemical engineering