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A new organic-inorganic hybrid strandberg structure polyoxometalate:{[Cu(phen)_2][Cu(phen)(H_2O)]_2P_2Mo_5O_(23)}·6H_2O

Meng Xianggao

Abstract

A new organic-inorganic hybrid polyoxometalate {[Cu(phen)2][Cu(phen)(H2O)]2P2Mo5O23}·6H2O has been hydrothermally synthesized,and characterized by element analysis,IR,TG analysis,and single-crystal X-ray diffraction.The compound crystallizes in the triclinic system,space group P1-,a=1.224 54(2)nm,b=1.435 86(14)nm,c=2.009 3(2)nm,α=80.192(2)°,β=74.585(2)°,γ=67.025(2)°,V=3.126 7(5)nm3,Z=2.

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Key concepts: Polyoxometalate, Crystallography, Chemistry, Materials science, Organic chemistry, Catalysis