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Synthesis and crystal structure of [Ni(C_8H_4O_4)(C_(12)H_(30)-N_6)]

Mei Wen-jie

Abstract

A novel nickel(Ⅱ) complex [Ni(C8H4O4)(C12H30N6)] had been synthesized and characterized by the single-crystal X-ray diffraction method.The results showed that the complex crystallized in a triclinic system,forming the space group P1 with a=7.581 8(5)?,b=8.397 6(5)?,c=9.759 6(6)?,α=105.506(1)°,β=97.283(1)°,γ=105.853(1)°,V=562.45(6)?3,Z=1,F(000)=256,Dc=1.421 g/cm3,R1=0.030,and wR2=0.081.The complex adopted a linear chain structure and the chains were all parallel.

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Key concepts: Triclinic crystal system, Chemistry, Crystallography, Crystal structure, Nickel, Chain (unit), Single crystal, Diffraction