Components Comparison of Essential Oil Extracted from Schisandrae Sphenantherae Fructus by Supercritical Fluid CO_2 Extraction and Steam Distillation
Liuqing Yang
Abstract
Liuqing Yang
Abstract
Objective To compare the different chemical constituents of essential oil from Schisandrae Sphenantherae Fractus extracted by supercritical ?uid CO2 extraction(SFE-CO2) and steam distillation(SD).Methods The orthogonal test was carried out to determine the optimal extraction conditions according to the yield of essential oil extracted by SFE-CO2.The SFE-CO2 and SD were used to extract essential oil which was identified by GC-MS.Results The optimal SFE-CO2 extraction conditions were as follows: The extraction temperature was 40 ℃,with extraction pressure 15 Mpa and extraction time 3 hours.The average extraction rate of the essential oil by SFE-CO2 and SD were 8.2 % and 1.4 %,and 16 and 24 components were identified by GC-MS analysis,respectively.Conclusion The results indicated that the average extraction rate of essential oil by SFE-CO2 was higher than that by SD,and both the components and content of the oil were different.
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Objective To compare the different chemical constituents of essential oil from Schisandrae Sphenantherae Fractus extracted by supercritical ?uid CO2 extraction(SFE-CO2) and steam distillation(SD).Methods The orthogonal test was carried out to determine the optimal extraction conditions according to the yield of essential oil extracted by SFE-CO2.The SFE-CO2 and SD were used to extract essential oil which was identified by GC-MS.Results The optimal SFE-CO2 extraction conditions were as follows: The extraction temperature was 40 ℃,with extraction pressure 15 Mpa and extraction time 3 hours.The average extraction rate of the essential oil by SFE-CO2 and SD were 8.2 % and 1.4 %,and 16 and 24 components were identified by GC-MS analysis,respectively.Conclusion The results indicated that the average extraction rate of essential oil by SFE-CO2 was higher than that by SD,and both the components and content of the oil were different.
Key concepts: Steam distillation, Chromatography, Extraction (chemistry), Chemistry, Supercritical fluid, Essential oil, Supercritical fluid extraction, Distillation