GC-MS Analysis of Essential Oil Components from Flowers of Edgeworthia chrysantha Lindl.
Ping Wu
Abstract
Ping Wu
Abstract
The chemical components of essential oil from the flowers of Edgeworthia chrysantha Lindl.were analyzed by GC-MS in this paper.Methods:The volatile components was extracted by diethyl e- ther,then isolated by steam distillation method.Their chemical compositions and relative contents were analyzed by GC-MS with HP-55% phenyl methyl siloxane capillary column(30m×0.25 mm×0.25μm).The carry- ing gas was helium,the flow rate was 1 mL·min~(-1) and the temperature was in rate of 8℃·min~(-1) from 30℃ (hold 5 min) to 120℃,then in rate of 20℃·min~(-1) from 120℃ to 240℃ (kept 10 min).Results:Sixty- one volatile compounds of Flos Edgeworthlae were identified,which comprised 60.14% of volatile fraction.One nitrogenous configurations;decane,1,1′-oxybis-;7-pentadecene 7-bromomethyl-and tert-hexadecanethi- ol were especial components.Conclusion:The method is reliable,stabilize and reproducible,therefore this meth- od can be applied to the analysis of the essential oil components,which was extracted from Flos Edgeworthlae components.
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The chemical components of essential oil from the flowers of Edgeworthia chrysantha Lindl.were analyzed by GC-MS in this paper.Methods:The volatile components was extracted by diethyl e- ther,then isolated by steam distillation method.Their chemical compositions and relative contents were analyzed by GC-MS with HP-55% phenyl methyl siloxane capillary column(30m×0.25 mm×0.25μm).The carry- ing gas was helium,the flow rate was 1 mL·min~(-1) and the temperature was in rate of 8℃·min~(-1) from 30℃ (hold 5 min) to 120℃,then in rate of 20℃·min~(-1) from 120℃ to 240℃ (kept 10 min).Results:Sixty- one volatile compounds of Flos Edgeworthlae were identified,which comprised 60.14% of volatile fraction.One nitrogenous configurations;decane,1,1′-oxybis-;7-pentadecene 7-bromomethyl-and tert-hexadecanethi- ol were especial components.Conclusion:The method is reliable,stabilize and reproducible,therefore this meth- od can be applied to the analysis of the essential oil components,which was extracted from Flos Edgeworthlae components.
Key concepts: Chemistry, Steam distillation, Chromatography, Essential oil, Flos, Fraction (chemistry), Decane, Gas chromatography–mass spectrometry