2006Shipin yanjiu yu kaifaRequires access

SYNTHESIS ETHHYL PROPIONATE CATALYZED BY SODIUM HYDROGEN SULFAT UNDER MICROWAVE IRRADIATION

Lan Xiang-rong

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Abstract

With propanoic acid and ethanol as raw materials,cyclohexane as water entrainer and sodium hydrogen sulfat as catalyst,ethhyl propionate was synthesized directly under normal pressure and microwave irradiation. The mole ratio of ethanol and propanoic acid was 2.5∶1.0,the amount of cyclohexane was 5 mL,the amount of sodium hydrogen sulfat was 0.3 g,and the microwave irradiation time was 8 min with the power of 665 W. The rate of esterification was over 98 %.

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What this paper is about

With propanoic acid and ethanol as raw materials,cyclohexane as water entrainer and sodium hydrogen sulfat as catalyst,ethhyl propionate was synthesized directly under normal pressure and microwave irradiation. The mole ratio of ethanol and propanoic acid was 2.5∶1.0,the amount of cyclohexane was 5 mL,the amount of sodium hydrogen sulfat was 0.3 g,and the microwave irradiation time was 8 min with the power of 665 W. The rate of esterification was over 98 %.

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Available abstract

With propanoic acid and ethanol as raw materials,cyclohexane as water entrainer and sodium hydrogen sulfat as catalyst,ethhyl propionate was synthesized directly under normal pressure and microwave irradiation. The mole ratio of ethanol and propanoic acid was 2.5∶1.0,the amount of cyclohexane was 5 mL,the amount of sodium hydrogen sulfat was 0.3 g,and the microwave irradiation time was 8 min with the power of 665 W. The rate of esterification was over 98 %.

Key concepts: Chemistry, Propanoic acid, Catalysis, Cyclohexane, Ethanol, Propionate, Sodium propionate, Nuclear chemistry

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