2003Chemical Research and ApplicationRequires access

Catalytic synthesis of iso-amyl propionate by ferric sulphate

Xiao‐Ping Song

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Abstract

Solid acid ferric sulphate Fe_2(SO_4)_3 was prepared and used for the study of the catalytic synthesis of iso-amyl propionate.The optimun reaction conditions were follows:the ratio of amount of substance n(iso-amylalcohol):n(propionic acid)=1.5,the reaction time 2h,the catalyst quantity 1.5g,and dewatering solvent toluene 10ml.The yield was 97.2% under the optimum reaction conditions.The catalyst being of high catalytic activity for the esterification reactions was prepared very easily and could be used repeatedly.

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Solid acid ferric sulphate Fe_2(SO_4)_3 was prepared and used for the study of the catalytic synthesis of iso-amyl propionate.The optimun reaction conditions were follows:the ratio of amount of substance n(iso-amylalcohol):n(propionic acid)=1.5,the reaction time 2h,the catalyst quantity 1.5g,and dewatering solvent toluene 10ml.The yield was 97.2% under the optimum reaction conditions.The catalyst being of high catalytic activity for the esterification reactions was prepared very easily and could be used repeatedly.

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Available abstract

Solid acid ferric sulphate Fe_2(SO_4)_3 was prepared and used for the study of the catalytic synthesis of iso-amyl propionate.The optimun reaction conditions were follows:the ratio of amount of substance n(iso-amylalcohol):n(propionic acid)=1.5,the reaction time 2h,the catalyst quantity 1.5g,and dewatering solvent toluene 10ml.The yield was 97.2% under the optimum reaction conditions.The catalyst being of high catalytic activity for the esterification reactions was prepared very easily and could be used repeatedly.

Key concepts: Catalysis, Chemistry, Propionate, Ferric, Yield (engineering), Toluene, Propionates, Solvent

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