Synthesis and Structural Characterization of New Calix[4] Arene Derivative
Pan Xian-jun
Abstract
Pan Xian-jun
Abstract
Firstly,the p-tert-butyl calix[4] arene was synthesized by one-step reaction of p-tert-phenol with formaldehyde.Then,a new compound,p-tert-butyl-25,27-dihydroxy-26,28-di(hydroxyethoxy) calix[4] arene,was obtained by the reaction of p-tert-butyl calix[4] arene with iodoethanol.The structure of the new compound was characterized with ~1H NMR,~(13)C NMR,IR,MS and element analysis.
A significance statement is not available in the OpenAlex record.
A contribution statement is not available in the OpenAlex record.
Method details are not available in the OpenAlex metadata.
Findings are not separately available in the OpenAlex metadata.
Limitations are not available in the OpenAlex metadata.
Application details are not available in the OpenAlex metadata.
Firstly,the p-tert-butyl calix[4] arene was synthesized by one-step reaction of p-tert-phenol with formaldehyde.Then,a new compound,p-tert-butyl-25,27-dihydroxy-26,28-di(hydroxyethoxy) calix[4] arene,was obtained by the reaction of p-tert-butyl calix[4] arene with iodoethanol.The structure of the new compound was characterized with ~1H NMR,~(13)C NMR,IR,MS and element analysis.
Key concepts: Formaldehyde, Calixarene, Phenol, Derivative (finance), Chemistry, Proton NMR, Stereochemistry, Organic chemistry