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2013•Guangzhou Chemical IndustryRequires access

Synthesis,Characterization and Crystal Structure of Waugh-type (C_7H_7N_2)_5Mn_(0.5)(H_2O)_2[MnMo_9O_(32)]·10H_2O Complex

Yao Zhang

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Abstract

The new Waugh molybdate was obtained by reacting of(NH4)6MnMo9O32·6H2O and benzimidazole in aqueous solution,and the structure and properties were characterized through single X-ray diffraction,IR,DRS and TG.The salt crystallized in the monoclnic space group a=10.813(6),b=15.848(9),c=36.395(2),β=95.143(10)°,V=6211.8.5(6)3,Z=2,Dc=9.841 g·cm-3,R1=0.0455,wR2=0.1005(I2σ),and GOF=1.032.

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What this paper is about

The new Waugh molybdate was obtained by reacting of(NH4)6MnMo9O32·6H2O and benzimidazole in aqueous solution,and the structure and properties were characterized through single X-ray diffraction,IR,DRS and TG.The salt crystallized in the monoclnic space group a=10.813(6),b=15.848(9),c=36.395(2),β=95.143(10)°,V=6211.8.5(6)3,Z=2,Dc=9.841 g·cm-3,R1=0.0455,wR2=0.1005(I2σ),and GOF=1.032.

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Available abstract

The new Waugh molybdate was obtained by reacting of(NH4)6MnMo9O32·6H2O and benzimidazole in aqueous solution,and the structure and properties were characterized through single X-ray diffraction,IR,DRS and TG.The salt crystallized in the monoclnic space group a=10.813(6),b=15.848(9),c=36.395(2),β=95.143(10)°,V=6211.8.5(6)3,Z=2,Dc=9.841 g·cm-3,R1=0.0455,wR2=0.1005(I2σ),and GOF=1.032.

Key concepts: Benzimidazole, Crystal structure, Crystallography, Molybdate, Chemistry, Aqueous solution, Salt (chemistry), Stereochemistry

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Synthesis,Characterization and Crystal Structure of Waugh-type (C_7H_7N_2)_5Mn_(0.5)(H_2O)_2[MnMo_9O_(32)]·10H_2O Complex — Research Paper | ScholarLens