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2011•Journal of Tonghua Normal UniversityRequires access

Hydrothermal Synthesis and Crystal Structure of a Cobalt(II) Polymer with One-dimensional Chain-like Structure:[Co(tdc)(phen)(H_2O)]_n

Xiu Li

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Abstract

A metal-organic coordination compound formulated as [Co(tdc)(phen)(H2O)]n 1(H2tdc = thiophene-2,5-dicarboxylic acid,phen =1,10-phenanthroline) has been hydrothermally synthesized and structurally characterized by elemental analysis,IR,TG and single-crystal X-ray diffraction.The compound crystallizes in the monoclinic system,space group P21/n with a = 1.0916(2),b = 1.5713(3),c = 1.1333(3) nm,β = 115.943(4)°,V=1.7480(7)nm3,C18H12CoN2O5S,Mr=427.29,Dc=1.624g/,μ(MoKα)=1.135mm-1,F(000)=868,Z=4,the final R = 0.0458 and wR = 0.0941 for 2445 observed reflections(I 2σ(I)).

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A metal-organic coordination compound formulated as [Co(tdc)(phen)(H2O)]n 1(H2tdc = thiophene-2,5-dicarboxylic acid,phen =1,10-phenanthroline) has been hydrothermally synthesized and structurally characterized by elemental analysis,IR,TG and single-crystal X-ray diffraction.The compound crystallizes in the monoclinic system,space group P21/n with a = 1.0916(2),b = 1.5713(3),c = 1.1333(3) nm,β = 115.943(4)°,V=1.7480(7)nm3,C18H12CoN2O5S,Mr=427.29,Dc=1.624g/,μ(MoKα)=1.135mm-1,F(000)=868,Z=4,the final R = 0.0458 and wR = 0.0941 for 2445 observed reflections(I 2σ(I)).

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Available abstract

A metal-organic coordination compound formulated as [Co(tdc)(phen)(H2O)]n 1(H2tdc = thiophene-2,5-dicarboxylic acid,phen =1,10-phenanthroline) has been hydrothermally synthesized and structurally characterized by elemental analysis,IR,TG and single-crystal X-ray diffraction.The compound crystallizes in the monoclinic system,space group P21/n with a = 1.0916(2),b = 1.5713(3),c = 1.1333(3) nm,β = 115.943(4)°,V=1.7480(7)nm3,C18H12CoN2O5S,Mr=427.29,Dc=1.624g/,μ(MoKα)=1.135mm-1,F(000)=868,Z=4,the final R = 0.0458 and wR = 0.0941 for 2445 observed reflections(I 2σ(I)).

Key concepts: Monoclinic crystal system, Crystallography, Cobalt, Hydrothermal synthesis, Hydrothermal circulation, Crystal structure, Thiophene, Coordination polymer

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