Study on the reaction of α-ketohemithioacetal with semicarbazide and thiosemicarbazide
He Ming Xiao
Abstract
He Ming Xiao
Abstract
The reaction of α ketohemithioacetal with semicarbazide and thiosemicarbazide were studied. The mono or disemicarbazone can be obtained by the control of the ratio of α ketohemithioacetal and semicarbazide. The same result was obtained from the reaction of thiosemicarbazide. The structure of products were confirmed by IR, NMR, MS and elemental analysis.
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The reaction of α ketohemithioacetal with semicarbazide and thiosemicarbazide were studied. The mono or disemicarbazone can be obtained by the control of the ratio of α ketohemithioacetal and semicarbazide. The same result was obtained from the reaction of thiosemicarbazide. The structure of products were confirmed by IR, NMR, MS and elemental analysis.
Key concepts: Semicarbazide, Chemistry, Molar ratio, Reaction conditions, Combinatorial chemistry, Elemental analysis, Nuclear chemistry, Organic chemistry