Study on preparation of MOS-Fe
XU Mu-dan
Abstract
XU Mu-dan
Abstract
In this paper, the effects of four factors: pH, reaction time, concentration of FeCl3, concentration of sodium citrate on the preparation of MOS-Fe were determined by orthogonal experiment. The optimum process conditions including the pH was 9, the reaction time was 1.5 h, the concentration of FeCl3 was 0.45 mol/L, and the concentration of sodium citrate was 0.20 mol/L. Determination of iron which is 1,10-phenanthroline was detected. And the IR, UV scanning to determine its structure.
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In this paper, the effects of four factors: pH, reaction time, concentration of FeCl3, concentration of sodium citrate on the preparation of MOS-Fe were determined by orthogonal experiment. The optimum process conditions including the pH was 9, the reaction time was 1.5 h, the concentration of FeCl3 was 0.45 mol/L, and the concentration of sodium citrate was 0.20 mol/L. Determination of iron which is 1,10-phenanthroline was detected. And the IR, UV scanning to determine its structure.
Key concepts: Sodium citrate, Chemistry, Sodium, Nuclear chemistry, Reaction conditions, Inorganic chemistry, Catalysis, Organic chemistry