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Ultrasonic-aided Ammonium Oxalate Extraction of Pectin from Promma microphylla Turcz Leaves

Jinling He

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Abstract

In the present study,ultrasonic radiation was found to largely enhance the extraction of pectin from Promma microphylla Turcz leaves with ammonium oxalate solution.In order to further intensify pectin extraction,the ultrasonic-aided ammonium oxalate extraction process was optimized by orthogonal array design on the basis of a series of single-factor experiments.Under the conditions studied,temperature,length of extraction time,ammonium oxalate concentration and mate-rial-to-liquid ratio could affect pectin extraction differently,and the effects of ammonium oxalate concentration and temperature were significant,and the optimal conditions of the four parameters were 70 ℃,70 min,8 g/L and 50:1,respectively.Under these conditions,the extraction rate of pectin reached up to 63.79%.Furthermore,the quality indicators of the extracted pectin could meet the requirements of the industrial standard(QB 2484-2000).

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What this paper is about

In the present study,ultrasonic radiation was found to largely enhance the extraction of pectin from Promma microphylla Turcz leaves with ammonium oxalate solution.In order to further intensify pectin extraction,the ultrasonic-aided ammonium oxalate extraction process was optimized by orthogonal array design on the basis of a series of single-factor experiments.Under the conditions studied,temperature,length of extraction time,ammonium oxalate concentration and mate-rial-to-liquid ratio could affect pectin extraction differently,and the effects of ammonium oxalate concentration and temperature were significant,and the optimal conditions of the four parameters were 70 ℃,70 min,8 g/L and 50:1,respectively.Under these conditions,the extraction rate of pectin reached up to 63.79%.Furthermore,the quality indicators of the extracted pectin could meet the requirements of the industrial standard(QB 2484-2000).

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Available abstract

In the present study,ultrasonic radiation was found to largely enhance the extraction of pectin from Promma microphylla Turcz leaves with ammonium oxalate solution.In order to further intensify pectin extraction,the ultrasonic-aided ammonium oxalate extraction process was optimized by orthogonal array design on the basis of a series of single-factor experiments.Under the conditions studied,temperature,length of extraction time,ammonium oxalate concentration and mate-rial-to-liquid ratio could affect pectin extraction differently,and the effects of ammonium oxalate concentration and temperature were significant,and the optimal conditions of the four parameters were 70 ℃,70 min,8 g/L and 50:1,respectively.Under these conditions,the extraction rate of pectin reached up to 63.79%.Furthermore,the quality indicators of the extracted pectin could meet the requirements of the industrial standard(QB 2484-2000).

Key concepts: Ammonium oxalate, Pectin, Extraction (chemistry), Ammonium, Oxalate, Chemistry, Chromatography, Ultrasonic sensor

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