Hydrothermal Synthesis and Crystal Structure of [Co(C_5O_2H_8)_2]·H_3COH
Xia Jin
Abstract
Xia Jin
Abstract
A novel complex[Co(C5O2H8)2]·H3COH was synthesized,the crystal structure of which was analyzed by X-ray diffraction.The crystal is monoclinic crystal with space group of P2(1)/c,and cell parameters are follow:a=0.93325(16)nm,b=1.15015(16)nm,c=1.30029(16)nm,α=90.00°,γ=90.00°,β=92.9680(10)°,V=1.3938(4)nm3,Z=4,Dc=1.388g·cm-3,F(000)=612;R1=0.0581,wR2=0.1700 and R1=0.0676,wR2=0.1786.
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A novel complex[Co(C5O2H8)2]·H3COH was synthesized,the crystal structure of which was analyzed by X-ray diffraction.The crystal is monoclinic crystal with space group of P2(1)/c,and cell parameters are follow:a=0.93325(16)nm,b=1.15015(16)nm,c=1.30029(16)nm,α=90.00°,γ=90.00°,β=92.9680(10)°,V=1.3938(4)nm3,Z=4,Dc=1.388g·cm-3,F(000)=612;R1=0.0581,wR2=0.1700 and R1=0.0676,wR2=0.1786.
Key concepts: Hydrothermal circulation, Crystal structure, Hydrothermal synthesis, Chemistry, Crystallography, Chemical engineering, Materials science, Engineering