GC-MS Determination of Fat-Soluble Components in Bark of Toona Sinensis
Zhang Zhen
Abstract
Zhang Zhen
Abstract
Sample of bark of Toona sinensis was extracted with ethanol and purified by passing through silica gel column.The fat-soluble components in the eluant were separated and identified by GC-MS,and their relative contents(in %) were found by the method of normalization.Totally 41 compounds were identified and determined,amounting to 91.99% of the total peak areas of the fat-soluble components.The main compounds found with their relative contents were as follows: terpenoids(36.58%),alkanes(31.70%) and fatty acid(21.95%).
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Sample of bark of Toona sinensis was extracted with ethanol and purified by passing through silica gel column.The fat-soluble components in the eluant were separated and identified by GC-MS,and their relative contents(in %) were found by the method of normalization.Totally 41 compounds were identified and determined,amounting to 91.99% of the total peak areas of the fat-soluble components.The main compounds found with their relative contents were as follows: terpenoids(36.58%),alkanes(31.70%) and fatty acid(21.95%).
Key concepts: Chemistry, Chromatography, Terpenoid, Bark (sound), Gas chromatography–mass spectrometry, Elution, Fatty acid, Silica gel