2007Natural Gas Chemical IndustryRequires access

The Simultaneous Determination of Benzaldehyde,Benzyl Alcohol and Benzoic Acid by Gas Chromatography

Bin Liang

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Abstract

A specific GC analysis method was established for the rapid quantification of the main products of liquid-phase oxidation of toluene,namely,benzaldehyde,benzyl alcohol and benzoic acid.A GC equipped with a FFAP capillary and a FID detector was adopted.O-nitrotoluene and dimethylphthalate were used as internal standards of benzaldehyde,benzyl alcohol and benzoic acid respectively.The results indicated that the mean recovery rate for spiked samples are 105.39%,101.94%,97.18%,respectively,and the standard deviations are 3.19%,3.71%,1.66%,respectively.

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What this paper is about

A specific GC analysis method was established for the rapid quantification of the main products of liquid-phase oxidation of toluene,namely,benzaldehyde,benzyl alcohol and benzoic acid.A GC equipped with a FFAP capillary and a FID detector was adopted.O-nitrotoluene and dimethylphthalate were used as internal standards of benzaldehyde,benzyl alcohol and benzoic acid respectively.The results indicated that the mean recovery rate for spiked samples are 105.39%,101.94%,97.18%,respectively,and the standard deviations are 3.19%,3.71%,1.66%,respectively.

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Available abstract

A specific GC analysis method was established for the rapid quantification of the main products of liquid-phase oxidation of toluene,namely,benzaldehyde,benzyl alcohol and benzoic acid.A GC equipped with a FFAP capillary and a FID detector was adopted.O-nitrotoluene and dimethylphthalate were used as internal standards of benzaldehyde,benzyl alcohol and benzoic acid respectively.The results indicated that the mean recovery rate for spiked samples are 105.39%,101.94%,97.18%,respectively,and the standard deviations are 3.19%,3.71%,1.66%,respectively.

Key concepts: Benzaldehyde, Benzyl alcohol, Benzoic acid, Toluene, Chemistry, Chromatography, Benzyl benzoate, Gas chromatography

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