Synthesis of Dimethyl N-Cyanodithioiminocarbonate in Aqueous Phase
Xiang Fu
Abstract
Xiang Fu
Abstract
Dimethyl N-cyanodithioiminocarbonate was facilely synthesized from calcium cyanamide, sodium carbonate and carbon disulfide, using dimethyl sulfate as a methylating agent in aqueous phase with an overall yield of 72% and purity of 99%.
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Dimethyl N-cyanodithioiminocarbonate was facilely synthesized from calcium cyanamide, sodium carbonate and carbon disulfide, using dimethyl sulfate as a methylating agent in aqueous phase with an overall yield of 72% and purity of 99%.
Key concepts: Chemistry, Dimethyl carbonate, Dimethyl sulfate, Cyanamide, Aqueous solution, Yield (engineering), Carbon disulfide, Sodium carbonate