ScholarLens Back to search
2009•Hecheng huaxueRequires access

Catalytic Synthesis of Polytetrahydrofuran by Phosphotungstic Heteropoly Acid Supported on Mesoporous Silica

Luo Shi-zhong

Open publisher page 0 citations

Abstract

The catalysts of phosphotungstic heteropoly acid(PW12) supported on silica(SiO2),PW12/SiO2,were prepared by impregnation method.The effect of PW12 loading amount[w(PW12)]and calcinated temperature on the catalytic activity of PW12/SiO2 were investigated.The results showed that the optimal catalyst(35Cat) was prepared under the conditions with w(PW12) of 35.0% and calcination at 230 ℃ for 3 h;the yield of PTHF reached 60.2% using 35Cat as a catalyst when the 35Cat percent in reactants tatol mass was 15.0%.

About this research paper

What this paper is about

The catalysts of phosphotungstic heteropoly acid(PW12) supported on silica(SiO2),PW12/SiO2,were prepared by impregnation method.The effect of PW12 loading amount[w(PW12)]and calcinated temperature on the catalytic activity of PW12/SiO2 were investigated.The results showed that the optimal catalyst(35Cat) was prepared under the conditions with w(PW12) of 35.0% and calcination at 230 ℃ for 3 h;the yield of PTHF reached 60.2% using 35Cat as a catalyst when the 35Cat percent in reactants tatol mass was 15.0%.

Why it matters

A significance statement is not available in the OpenAlex record.

Key contribution

A contribution statement is not available in the OpenAlex record.

Method / approach

Method details are not available in the OpenAlex metadata.

Main findings

Findings are not separately available in the OpenAlex metadata.

Limitations

Limitations are not available in the OpenAlex metadata.

Applications

Application details are not available in the OpenAlex metadata.

Available abstract

The catalysts of phosphotungstic heteropoly acid(PW12) supported on silica(SiO2),PW12/SiO2,were prepared by impregnation method.The effect of PW12 loading amount[w(PW12)]and calcinated temperature on the catalytic activity of PW12/SiO2 were investigated.The results showed that the optimal catalyst(35Cat) was prepared under the conditions with w(PW12) of 35.0% and calcination at 230 ℃ for 3 h;the yield of PTHF reached 60.2% using 35Cat as a catalyst when the 35Cat percent in reactants tatol mass was 15.0%.

Key concepts: Phosphotungstic acid, Catalysis, Chemistry, Calcination, Yield (engineering), Mesoporous material, Heteropoly acid, Mesoporous silica

Related papers

Related paper 1Related paper 2Related paper 3
Back to paper searchBrowse research topicsOriginal source
Catalytic Synthesis of Polytetrahydrofuran by Phosphotungstic Heteropoly Acid Supported on Mesoporous Silica — Research Paper | ScholarLens