Determination of Dimetachlone Residues in Tomato and Soil by HPLC
Li Xie
Abstract
Li Xie
Abstract
The HPLC method for determination the residue of dimetachlone in tomato and soil simultaneously was developed.[Methods] The residues were extracted from samples with acetone,extracted by dichloromethane,purified by florisil column,and finally detected by HPLC.[Results] Good linearity was obtained in range from 0.010?52 to 5.26 mg/L.The minimum detectable concentration of dimetachlone in tomato and soil sample were both 0.05 mg/kg.The recovery rate were 79.97-109.84%.The variation coefficient were 1.91-10.55% respectively.[Conclusions] The study results indicated that the sensitivity and precision of this method both meet the technical requirements of the residual analysis.
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The HPLC method for determination the residue of dimetachlone in tomato and soil simultaneously was developed.[Methods] The residues were extracted from samples with acetone,extracted by dichloromethane,purified by florisil column,and finally detected by HPLC.[Results] Good linearity was obtained in range from 0.010?52 to 5.26 mg/L.The minimum detectable concentration of dimetachlone in tomato and soil sample were both 0.05 mg/kg.The recovery rate were 79.97-109.84%.The variation coefficient were 1.91-10.55% respectively.[Conclusions] The study results indicated that the sensitivity and precision of this method both meet the technical requirements of the residual analysis.
Key concepts: Chromatography, Residue (chemistry), Chemistry, High-performance liquid chromatography, Dichloromethane, Acetone, Coefficient of variation, Soil test