2013•Unpublished venueRequires access

Determination of Dimetachlone Residues in Tomato and Soil by HPLC

Li Xie

Open publisher page 1 citations

Abstract

The HPLC method for determination the residue of dimetachlone in tomato and soil simultaneously was developed.[Methods] The residues were extracted from samples with acetone,extracted by dichloromethane,purified by florisil column,and finally detected by HPLC.[Results] Good linearity was obtained in range from 0.010?52 to 5.26 mg/L.The minimum detectable concentration of dimetachlone in tomato and soil sample were both 0.05 mg/kg.The recovery rate were 79.97-109.84%.The variation coefficient were 1.91-10.55% respectively.[Conclusions] The study results indicated that the sensitivity and precision of this method both meet the technical requirements of the residual analysis.

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The HPLC method for determination the residue of dimetachlone in tomato and soil simultaneously was developed.[Methods] The residues were extracted from samples with acetone,extracted by dichloromethane,purified by florisil column,and finally detected by HPLC.[Results] Good linearity was obtained in range from 0.010?52 to 5.26 mg/L.The minimum detectable concentration of dimetachlone in tomato and soil sample were both 0.05 mg/kg.The recovery rate were 79.97-109.84%.The variation coefficient were 1.91-10.55% respectively.[Conclusions] The study results indicated that the sensitivity and precision of this method both meet the technical requirements of the residual analysis.

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Available abstract

The HPLC method for determination the residue of dimetachlone in tomato and soil simultaneously was developed.[Methods] The residues were extracted from samples with acetone,extracted by dichloromethane,purified by florisil column,and finally detected by HPLC.[Results] Good linearity was obtained in range from 0.010?52 to 5.26 mg/L.The minimum detectable concentration of dimetachlone in tomato and soil sample were both 0.05 mg/kg.The recovery rate were 79.97-109.84%.The variation coefficient were 1.91-10.55% respectively.[Conclusions] The study results indicated that the sensitivity and precision of this method both meet the technical requirements of the residual analysis.

Key concepts: Chromatography, Residue (chemistry), Chemistry, High-performance liquid chromatography, Dichloromethane, Acetone, Coefficient of variation, Soil test

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