2015Anhui nongye kexueRequires access

Microwave Digestion,ICP-oa TOF-MS Method for the Determination of Ten Elements in Teas

He Ji

Open publisher page 0 citations

Abstract

[Objective]To investigate pre-treatment by hermetic microwave digestion and feasibility of determination 10 elements in tea by using ICP-oa TOF-MS. [Method] A method was used to determination 10 elementss in tea by using ICP-oa TOF-MS after microwave digestion with nitrate- hydrogen peroxide,which was validated from the linearity,accuracy,precision and recovery rate. [Result] Results showed that 10 elements metal the requirements of real sample detection,with linear r 0. 999 5,RSD 4%,and recoveries 94. 00%- 103. 05%. [Conclusion]Compared with other methods,this method is a simple rapid determination multiple elements from tea samples and accurate high sensitivity. Especially for some low concentration of ng / L of the components of the level of trace detection.

About this research paper

What this paper is about

[Objective]To investigate pre-treatment by hermetic microwave digestion and feasibility of determination 10 elements in tea by using ICP-oa TOF-MS. [Method] A method was used to determination 10 elementss in tea by using ICP-oa TOF-MS after microwave digestion with nitrate- hydrogen peroxide,which was validated from the linearity,accuracy,precision and recovery rate. [Result] Results showed that 10 elements metal the requirements of real sample detection,with linear r 0. 999 5,RSD 4%,and recoveries 94. 00%- 103. 05%. [Conclusion]Compared with other methods,this method is a simple rapid determination multiple elements from tea samples and accurate high sensitivity. Especially for some low concentration of ng / L of the components of the level of trace detection.

Why it matters

A significance statement is not available in the OpenAlex record.

Key contribution

A contribution statement is not available in the OpenAlex record.

Method / approach

Method details are not available in the OpenAlex metadata.

Main findings

Findings are not separately available in the OpenAlex metadata.

Limitations

Limitations are not available in the OpenAlex metadata.

Applications

Application details are not available in the OpenAlex metadata.

Available abstract

[Objective]To investigate pre-treatment by hermetic microwave digestion and feasibility of determination 10 elements in tea by using ICP-oa TOF-MS. [Method] A method was used to determination 10 elementss in tea by using ICP-oa TOF-MS after microwave digestion with nitrate- hydrogen peroxide,which was validated from the linearity,accuracy,precision and recovery rate. [Result] Results showed that 10 elements metal the requirements of real sample detection,with linear r 0. 999 5,RSD 4%,and recoveries 94. 00%- 103. 05%. [Conclusion]Compared with other methods,this method is a simple rapid determination multiple elements from tea samples and accurate high sensitivity. Especially for some low concentration of ng / L of the components of the level of trace detection.

Key concepts: Microwave digestion, Chromatography, Chemistry, Detection limit, Hydrogen peroxide, Digestion (alchemy), Recovery rate, Inductively coupled plasma mass spectrometry

Related papers

Back to paper searchBrowse research topicsOriginal source
Microwave Digestion,ICP-oa TOF-MS Method for the Determination of Ten Elements in Teas — Research Paper | ScholarLens