Microwave Digestion,ICP-oa TOF-MS Method for the Determination of Ten Elements in Teas
He Ji
Abstract
He Ji
Abstract
[Objective]To investigate pre-treatment by hermetic microwave digestion and feasibility of determination 10 elements in tea by using ICP-oa TOF-MS. [Method] A method was used to determination 10 elementss in tea by using ICP-oa TOF-MS after microwave digestion with nitrate- hydrogen peroxide,which was validated from the linearity,accuracy,precision and recovery rate. [Result] Results showed that 10 elements metal the requirements of real sample detection,with linear r 0. 999 5,RSD 4%,and recoveries 94. 00%- 103. 05%. [Conclusion]Compared with other methods,this method is a simple rapid determination multiple elements from tea samples and accurate high sensitivity. Especially for some low concentration of ng / L of the components of the level of trace detection.
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[Objective]To investigate pre-treatment by hermetic microwave digestion and feasibility of determination 10 elements in tea by using ICP-oa TOF-MS. [Method] A method was used to determination 10 elementss in tea by using ICP-oa TOF-MS after microwave digestion with nitrate- hydrogen peroxide,which was validated from the linearity,accuracy,precision and recovery rate. [Result] Results showed that 10 elements metal the requirements of real sample detection,with linear r 0. 999 5,RSD 4%,and recoveries 94. 00%- 103. 05%. [Conclusion]Compared with other methods,this method is a simple rapid determination multiple elements from tea samples and accurate high sensitivity. Especially for some low concentration of ng / L of the components of the level of trace detection.
Key concepts: Microwave digestion, Chromatography, Chemistry, Detection limit, Hydrogen peroxide, Digestion (alchemy), Recovery rate, Inductively coupled plasma mass spectrometry