Synthesis of anthraquinone by oxidation with H_2O_2 under microwave irradiation
Kou Jia-hui
Abstract
Kou Jia-hui
Abstract
The oxidation of anthracene with H_2O_2 under microwave irradiation was investigated.The effects of reaction time,H_2O_2 feed,catalyst and solvent were examined.The results showed that anthraquinone yield was significantly affected by the concentration of acetic acid and that using proper amount of (CH_3COO)_3Fe as catalyst could increase the anthraquinone yield and shorten the reaction time.
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The oxidation of anthracene with H_2O_2 under microwave irradiation was investigated.The effects of reaction time,H_2O_2 feed,catalyst and solvent were examined.The results showed that anthraquinone yield was significantly affected by the concentration of acetic acid and that using proper amount of (CH_3COO)_3Fe as catalyst could increase the anthraquinone yield and shorten the reaction time.
Key concepts: Chemistry, Anthraquinone, Yield (engineering), Anthracene, Acetic acid, Catalysis, Microwave irradiation, Solvent