ScholarLens Back to search
2010•China ElastomericsRequires access

Catalytic synthesis of ditrimethylolpropane tetraacrylate(Di-TMPTA) over H_4SiW_(12)O_(40)/C

Zhang Ji-bo

Open publisher page 0 citations

Abstract

Di-TMPTA was synthesized from Di-TMP and acrylicacid by direct esterification method with H4SiW12O40/C as catalyst.The influence of reaction conditions were studied.The results indicated that the most suitable condition is as follows:mole ratio of crylic acid to Di-TMP was 4.0∶1,H4SiW12O40/C as the catalyst with 0.5%,reaction time was above 4 hours,the esterification rate of reaction was 96.5%.The product was qualitative analysised by IR.

About this research paper

What this paper is about

Di-TMPTA was synthesized from Di-TMP and acrylicacid by direct esterification method with H4SiW12O40/C as catalyst.The influence of reaction conditions were studied.The results indicated that the most suitable condition is as follows:mole ratio of crylic acid to Di-TMP was 4.0∶1,H4SiW12O40/C as the catalyst with 0.5%,reaction time was above 4 hours,the esterification rate of reaction was 96.5%.The product was qualitative analysised by IR.

Why it matters

A significance statement is not available in the OpenAlex record.

Key contribution

A contribution statement is not available in the OpenAlex record.

Method / approach

Method details are not available in the OpenAlex metadata.

Main findings

Findings are not separately available in the OpenAlex metadata.

Limitations

Limitations are not available in the OpenAlex metadata.

Applications

Application details are not available in the OpenAlex metadata.

Available abstract

Di-TMPTA was synthesized from Di-TMP and acrylicacid by direct esterification method with H4SiW12O40/C as catalyst.The influence of reaction conditions were studied.The results indicated that the most suitable condition is as follows:mole ratio of crylic acid to Di-TMP was 4.0∶1,H4SiW12O40/C as the catalyst with 0.5%,reaction time was above 4 hours,the esterification rate of reaction was 96.5%.The product was qualitative analysised by IR.

Key concepts: Catalysis, TMPTA, Materials science, Nuclear chemistry, Reaction conditions, Organic chemistry, Chemistry, Monomer

Related papers

Related paper 1Related paper 2Related paper 3
Back to paper searchBrowse research topicsOriginal source
Catalytic synthesis of ditrimethylolpropane tetraacrylate(Di-TMPTA) over H_4SiW_(12)O_(40)/C — Research Paper | ScholarLens