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2013•Chinese Journal of Spectroscopy LaboratoryRequires access

Hydrothermal Synthesis and Crystal Structure of 1,3,5-benzenetricarboxylic Acid Ni(II)Coordination Polymer

Wei Zhao

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Abstract

Three dimensional mesh of Ni(Ⅱ) Coordination Polymer was synthesized by hydrothermal reaction of NiCl2·6H2O and 1,3,5-benzenetricarboxylic acid as raw materials.The structure was characterized by elemental analysis and single crystal X-ray diffraction analysis.The results show that.The molecular formula Ni3O30C18H42,triclinic,space groupP-1(2),a=0.6698(3)nm,b=1.0771(4)nm,c=1.2323(5)nm,α=73.342(9)°,β=77.76(1)°,γ=71.76(1)°,V=801.59(57),D=1.982g·cm-3,F(000)=4500,Rgt(F)=0.0287,wRref(F2)=0.0809.

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Three dimensional mesh of Ni(Ⅱ) Coordination Polymer was synthesized by hydrothermal reaction of NiCl2·6H2O and 1,3,5-benzenetricarboxylic acid as raw materials.The structure was characterized by elemental analysis and single crystal X-ray diffraction analysis.The results show that.The molecular formula Ni3O30C18H42,triclinic,space groupP-1(2),a=0.6698(3)nm,b=1.0771(4)nm,c=1.2323(5)nm,α=73.342(9)°,β=77.76(1)°,γ=71.76(1)°,V=801.59(57),D=1.982g·cm-3,F(000)=4500,Rgt(F)=0.0287,wRref(F2)=0.0809.

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Available abstract

Three dimensional mesh of Ni(Ⅱ) Coordination Polymer was synthesized by hydrothermal reaction of NiCl2·6H2O and 1,3,5-benzenetricarboxylic acid as raw materials.The structure was characterized by elemental analysis and single crystal X-ray diffraction analysis.The results show that.The molecular formula Ni3O30C18H42,triclinic,space groupP-1(2),a=0.6698(3)nm,b=1.0771(4)nm,c=1.2323(5)nm,α=73.342(9)°,β=77.76(1)°,γ=71.76(1)°,V=801.59(57),D=1.982g·cm-3,F(000)=4500,Rgt(F)=0.0287,wRref(F2)=0.0809.

Key concepts: Triclinic crystal system, Hydrothermal reaction, Hydrothermal circulation, Crystal structure, Coordination polymer, Hydrothermal synthesis, Crystallography, Materials science

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Hydrothermal Synthesis and Crystal Structure of 1,3,5-benzenetricarboxylic Acid Ni(II)Coordination Polymer — Research Paper | ScholarLens