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Research on Synthesis Technology of Lactide by Lactic Acid

Qingning Wang

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Abstract

Intermediate product lactide was synthesized from lactic acid.The effects of reaction temperature,time,and catalyst on the synthesis were discussed by means of orthogonal experimentation,and the optimum condition was determined:the mass ratio of SnCl2·2H2O to lactic acid was 0.25,p-toluenesulfonic acid to lactic acid was 0.75,reacted at 150 ℃ for 4 h.Lactide yield could reach to 43.3% when 30ml n-octanol was added in the late of the reaction.

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Intermediate product lactide was synthesized from lactic acid.The effects of reaction temperature,time,and catalyst on the synthesis were discussed by means of orthogonal experimentation,and the optimum condition was determined:the mass ratio of SnCl2·2H2O to lactic acid was 0.25,p-toluenesulfonic acid to lactic acid was 0.75,reacted at 150 ℃ for 4 h.Lactide yield could reach to 43.3% when 30ml n-octanol was added in the late of the reaction.

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Available abstract

Intermediate product lactide was synthesized from lactic acid.The effects of reaction temperature,time,and catalyst on the synthesis were discussed by means of orthogonal experimentation,and the optimum condition was determined:the mass ratio of SnCl2·2H2O to lactic acid was 0.25,p-toluenesulfonic acid to lactic acid was 0.75,reacted at 150 ℃ for 4 h.Lactide yield could reach to 43.3% when 30ml n-octanol was added in the late of the reaction.

Key concepts: Lactic acid, Lactide, Yield (engineering), Catalysis, Materials science, Organic chemistry, Chemistry, Composite material

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