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2011•Journal of Tonghua Normal UniversityRequires access

Hydrothermal Synthesis and Crystal Structure of Cadmium(II) Coordination Polymer Assembled by Pyrazine-2,3-dicarboxylic Acid

Zhi‐Tao Wang

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Abstract

A one-dimensional coordination polymer,[Cd(pzdc)(H2O)3]n(H2pzdc= pyrazine-2,3-dicarboxylic acid) has been obtained by using hydrothermal synthesis and characterized by elemental analysis,IR spectrum and single-crystal X-ray diffraction.The compound crystallized in the orthorhombic system,space group P2(1)2(1)2(1) with a=5.7341(4),b=10.8279(7),c=15.3484(10),V=952.96(11)3,C6H8CdN2O7,Mr=332.54,Dc=2.318g/cm3,μ(MoKα)=2.317mm-1,F(000)=648,Z=4,R1=0.0162,wR2=0.0449.

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What this paper is about

A one-dimensional coordination polymer,[Cd(pzdc)(H2O)3]n(H2pzdc= pyrazine-2,3-dicarboxylic acid) has been obtained by using hydrothermal synthesis and characterized by elemental analysis,IR spectrum and single-crystal X-ray diffraction.The compound crystallized in the orthorhombic system,space group P2(1)2(1)2(1) with a=5.7341(4),b=10.8279(7),c=15.3484(10),V=952.96(11)3,C6H8CdN2O7,Mr=332.54,Dc=2.318g/cm3,μ(MoKα)=2.317mm-1,F(000)=648,Z=4,R1=0.0162,wR2=0.0449.

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Available abstract

A one-dimensional coordination polymer,[Cd(pzdc)(H2O)3]n(H2pzdc= pyrazine-2,3-dicarboxylic acid) has been obtained by using hydrothermal synthesis and characterized by elemental analysis,IR spectrum and single-crystal X-ray diffraction.The compound crystallized in the orthorhombic system,space group P2(1)2(1)2(1) with a=5.7341(4),b=10.8279(7),c=15.3484(10),V=952.96(11)3,C6H8CdN2O7,Mr=332.54,Dc=2.318g/cm3,μ(MoKα)=2.317mm-1,F(000)=648,Z=4,R1=0.0162,wR2=0.0449.

Key concepts: Orthorhombic crystal system, Pyrazine, Coordination polymer, Hydrothermal synthesis, Dicarboxylic acid, Crystallography, Hydrothermal circulation, Crystal structure

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Hydrothermal Synthesis and Crystal Structure of Cadmium(II) Coordination Polymer Assembled by Pyrazine-2,3-dicarboxylic Acid — Research Paper | ScholarLens