[Synthesis and characterization of chitosan-imine-palladacycle].
Pu Liu, Li Sanhua, Xiangyu Wang, Limin Li
Abstract
Pu Liu, Li Sanhua, Xiangyu Wang, Limin Li
Abstract
Chitosan was grafted with salicylaldehyde to obtain Schiff base. The Schiff base reacted with Li2 PdCl4 in methanol to synthesize chitosan-imine-palladacycle. The structure of chitosan, schiffbase and chitosan-imine-palladacycle was characterized by IR, XRD, DTA-TG, fluorescence and XPS. According to the results of analysis, the structure of Schiff base and chitosanimine-palladacycle can be inferred.
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Chitosan was grafted with salicylaldehyde to obtain Schiff base. The Schiff base reacted with Li2 PdCl4 in methanol to synthesize chitosan-imine-palladacycle. The structure of chitosan, schiffbase and chitosan-imine-palladacycle was characterized by IR, XRD, DTA-TG, fluorescence and XPS. According to the results of analysis, the structure of Schiff base and chitosanimine-palladacycle can be inferred.
Key concepts: Imine, Salicylaldehyde, Schiff base, Chitosan, Chemistry, Polymer chemistry, Methanol, Organic chemistry