Synthesis of Isoamyl Hexanoate with Phosphotungstic Acid Pure as Catalyst
Jizhong Li
Abstract
Jizhong Li
Abstract
Isoamyl hexanoate was synthesized with hexanoic acid and isopentanol as raw materials and phosphotungstic acid pure as the catalyst.The factors influencing reaction were investigated.Experimental results indicated that the optimum conditions of esterification reaction were the molar ratio of hexanoic acid and isopentanol and phosphotungstic acid 1∶3∶0.0023,the reaction time 40 min,and the yield got up to 98.92%.
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Isoamyl hexanoate was synthesized with hexanoic acid and isopentanol as raw materials and phosphotungstic acid pure as the catalyst.The factors influencing reaction were investigated.Experimental results indicated that the optimum conditions of esterification reaction were the molar ratio of hexanoic acid and isopentanol and phosphotungstic acid 1∶3∶0.0023,the reaction time 40 min,and the yield got up to 98.92%.
Key concepts: Hexanoic acid, Phosphotungstic acid, Chemistry, Isoamyl acetate, Ethyl hexanoate, Yield (engineering), Catalysis, Molar ratio