The Influence of High Energy Ball Milling Time on the Grain Size and Sintering Densification Behavior of W-30Cu Composite Powder
Shuang Hu
Abstract
Shuang Hu
Abstract
Grain size and sintering densification behavior of W-30Cu composite powder influenced by high energy milling time were investigated.The result shows that,while the high energy ball milling time was in the range of 16 ~ 33 h,the crystalline size of the composite powder was reduced from 25 nm to 10 nm,and the mechanical alloy phenomenon was happened;while sintered at 1 275 ℃ for 60 m the composite powder milled for 18 h was achieved 100% density.Likewise,the high energy ball milled W-30Cu composite powder has the excellent hot stabilization,while the composite powder was annealed at 950 ℃,the grain size was not coarsen;The hardness of the sintered W-30Cu composite material was higher than the normal.The W-30Cu composite with the grain size about 300 ~ 550 nm can be achieved after sintering at 1 275 ℃ for 30 min.
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Grain size and sintering densification behavior of W-30Cu composite powder influenced by high energy milling time were investigated.The result shows that,while the high energy ball milling time was in the range of 16 ~ 33 h,the crystalline size of the composite powder was reduced from 25 nm to 10 nm,and the mechanical alloy phenomenon was happened;while sintered at 1 275 ℃ for 60 m the composite powder milled for 18 h was achieved 100% density.Likewise,the high energy ball milled W-30Cu composite powder has the excellent hot stabilization,while the composite powder was annealed at 950 ℃,the grain size was not coarsen;The hardness of the sintered W-30Cu composite material was higher than the normal.The W-30Cu composite with the grain size about 300 ~ 550 nm can be achieved after sintering at 1 275 ℃ for 30 min.
Key concepts: Materials science, Composite number, Sintering, Ball mill, Grain size, Grain growth, Composite material, Metallurgy