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Synthesis of N-Acetyl Morpholine

HE Mei-qin

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Abstract

N-Acetyl morpholine was synthesized using acetic acid and morpholine as raw materials.The influencing factors including the mole ratio of acetic acid to morpholine,reaction temperature and dehydraing agent were investigated.The yield of N-acetyl morpholine reachs 91.5% in the existence of dehydrating agent,at temperature of 40～145°C,and with molar ratio of acetic acid: morpholine=0.95∶1.The purity of N-acetyl morpholine distillated is 98.5%.

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What this paper is about

N-Acetyl morpholine was synthesized using acetic acid and morpholine as raw materials.The influencing factors including the mole ratio of acetic acid to morpholine,reaction temperature and dehydraing agent were investigated.The yield of N-acetyl morpholine reachs 91.5% in the existence of dehydrating agent,at temperature of 40～145°C,and with molar ratio of acetic acid: morpholine=0.95∶1.The purity of N-acetyl morpholine distillated is 98.5%.

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Available abstract

N-Acetyl morpholine was synthesized using acetic acid and morpholine as raw materials.The influencing factors including the mole ratio of acetic acid to morpholine,reaction temperature and dehydraing agent were investigated.The yield of N-acetyl morpholine reachs 91.5% in the existence of dehydrating agent,at temperature of 40～145°C,and with molar ratio of acetic acid: morpholine=0.95∶1.The purity of N-acetyl morpholine distillated is 98.5%.

Key concepts: Morpholine, Chemistry, Acetic acid, Yield (engineering), Molar ratio, Organic chemistry, Nuclear chemistry, Catalysis

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