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Analysis of Volatile Components from Fennel Bean

Dan Liu

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Abstract

The volatile components of fennel bean were extracted by head space solid phase microextraction(HS-SPME) and analyzed by gas chromatography mass spectrometry(GC-MS).The optimum operating conditions for SPME were determined as following: head space adsorption at 55 ℃ for 60 min using a 75 μm Carboxen/PDMS fiber.A total of 38 compounds were identified,representing 86.87% of the total peak area and consisted of 15 hydrocarbons,13 aldehydes and ketones,3 alcohols,3 phenols,3 ethers and 4 other compounds.The prevailing compounds were 1-methoxy-4-(1-propenyl) benzene(40.75%),nonanal(4.16%),cis-anethole(3.77%),limonene(3.48%),and estragole(2.9%).

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What this paper is about

The volatile components of fennel bean were extracted by head space solid phase microextraction(HS-SPME) and analyzed by gas chromatography mass spectrometry(GC-MS).The optimum operating conditions for SPME were determined as following: head space adsorption at 55 ℃ for 60 min using a 75 μm Carboxen/PDMS fiber.A total of 38 compounds were identified,representing 86.87% of the total peak area and consisted of 15 hydrocarbons,13 aldehydes and ketones,3 alcohols,3 phenols,3 ethers and 4 other compounds.The prevailing compounds were 1-methoxy-4-(1-propenyl) benzene(40.75%),nonanal(4.16%),cis-anethole(3.77%),limonene(3.48%),and estragole(2.9%).

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Available abstract

The volatile components of fennel bean were extracted by head space solid phase microextraction(HS-SPME) and analyzed by gas chromatography mass spectrometry(GC-MS).The optimum operating conditions for SPME were determined as following: head space adsorption at 55 ℃ for 60 min using a 75 μm Carboxen/PDMS fiber.A total of 38 compounds were identified,representing 86.87% of the total peak area and consisted of 15 hydrocarbons,13 aldehydes and ketones,3 alcohols,3 phenols,3 ethers and 4 other compounds.The prevailing compounds were 1-methoxy-4-(1-propenyl) benzene(40.75%),nonanal(4.16%),cis-anethole(3.77%),limonene(3.48%),and estragole(2.9%).

Key concepts: Estragole, Chemistry, Nonanal, Chromatography, Limonene, Solid-phase microextraction, Gas chromatography–mass spectrometry, Heptanal

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