2009•Journal of Langfang Teachers CollegeRequires access

Study on Preparation of Solid Phosphoric Acid Catalyst used as a Catalyst to Synthesize Acetic Ether

Xi Zhang

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Abstract

Solid phosphoric acid catalyst was prepared by impregnation method and their catalytic activity for synthesizing ethyl acetate was investigated.The effects of varied factors in solid phosphoric acid preparation and esterification have been analyzed.The results of test indicate that the better reaction conditions are: When the amount of catalyst is 30%(based on mass of acetic acid) and the molar ratio of acetic acid to alcohol is 1:3,the yield can reach 70.3% after 2 hours.

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What this paper is about

Solid phosphoric acid catalyst was prepared by impregnation method and their catalytic activity for synthesizing ethyl acetate was investigated.The effects of varied factors in solid phosphoric acid preparation and esterification have been analyzed.The results of test indicate that the better reaction conditions are: When the amount of catalyst is 30%(based on mass of acetic acid) and the molar ratio of acetic acid to alcohol is 1:3,the yield can reach 70.3% after 2 hours.

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Available abstract

Solid phosphoric acid catalyst was prepared by impregnation method and their catalytic activity for synthesizing ethyl acetate was investigated.The effects of varied factors in solid phosphoric acid preparation and esterification have been analyzed.The results of test indicate that the better reaction conditions are: When the amount of catalyst is 30%(based on mass of acetic acid) and the molar ratio of acetic acid to alcohol is 1:3,the yield can reach 70.3% after 2 hours.

Key concepts: Phosphoric acid, Catalysis, Acetic acid, Solid acid, Yield (engineering), Molar ratio, Alcohol, Chemistry

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