2007•Tianjin Chemical IndustryRequires access
Catalytic synthesis of isoamyl hexanoate with heteropolyacid
Wang Shou-qing
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Abstract
Isoamyl hexanoate was synthesized using isoamyl alcohol and hexanoic acid catalyzed by Heteropolyacid. The optimium reation condition in synthesis of Isoamyl hexanoate catalyzed with Heteropolyacid were determined : alcohol/acid molar ratio 1.6∶1, reaction time 2 h, the amount of catalyst 0.8 g, the taking water reagent(cyclohexane)7.5 mL. Under this conditions, the yieid of Isoamyl hexanoate was up to 98.8%.