Catalytic Synthesis of Amyl Cinnamate by Potassium Bisulfare
Ling Shao-ming
Abstract
Ling Shao-ming
Abstract
Amyl cinnamate was synthesized by the esterifiestion of amyl alcohol with cinnamic acid in the presence of potassium bisulfate monohydrate.The best reaction conditions were as follows:the amount of substance ratio of cinnamic acid/ amyl alcohol /potassium bisulfate is 1∶9.4∶0.46,the time of reaction were 4h and the ester yield reached 90.1%.The potassium bisulfate monohydrate is a catalyst with fairly high catalytic activity of the esterification reaction,which can accelerate amyl cinnamate synthesis.At the same time,the potassium bisulfate monohydrate can be recovered and reused.
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Amyl cinnamate was synthesized by the esterifiestion of amyl alcohol with cinnamic acid in the presence of potassium bisulfate monohydrate.The best reaction conditions were as follows:the amount of substance ratio of cinnamic acid/ amyl alcohol /potassium bisulfate is 1∶9.4∶0.46,the time of reaction were 4h and the ester yield reached 90.1%.The potassium bisulfate monohydrate is a catalyst with fairly high catalytic activity of the esterification reaction,which can accelerate amyl cinnamate synthesis.At the same time,the potassium bisulfate monohydrate can be recovered and reused.
Key concepts: Potassium, Chemistry, Catalysis, Yield (engineering), Alcohol, Cinnamic acid, Organic chemistry, Medicinal chemistry