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Evaluation of uncertainty for detection of Quinolones residues in aquatic products by HPLC-MS/MS

Wei Bojuan, WU Cheng-ye, Qian Zhuo-zhen

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Abstract

We establish a mathematical model for evaluation of the uncertainty of detecting Quinolones residues in aquatic products by high performance liquid-MS/MS ( HPLC-MS/ MS) , and analyze the sources of uncertainty in determination. By calculating the compo- nents of all uncertainties, relative combined standard uncertainty and expand uncertainty, we obtain a report of uncertainty of Qinolo- nes. The results show that the main source of the uncertainty comes from HPLC-MS/MS and preparation of standard solution.

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What this paper is about

We establish a mathematical model for evaluation of the uncertainty of detecting Quinolones residues in aquatic products by high performance liquid-MS/MS ( HPLC-MS/ MS) , and analyze the sources of uncertainty in determination. By calculating the compo- nents of all uncertainties, relative combined standard uncertainty and expand uncertainty, we obtain a report of uncertainty of Qinolo- nes. The results show that the main source of the uncertainty comes from HPLC-MS/MS and preparation of standard solution.

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Available abstract

We establish a mathematical model for evaluation of the uncertainty of detecting Quinolones residues in aquatic products by high performance liquid-MS/MS ( HPLC-MS/ MS) , and analyze the sources of uncertainty in determination. By calculating the compo- nents of all uncertainties, relative combined standard uncertainty and expand uncertainty, we obtain a report of uncertainty of Qinolo- nes. The results show that the main source of the uncertainty comes from HPLC-MS/MS and preparation of standard solution.

Key concepts: Standard uncertainty, High-performance liquid chromatography, Measurement uncertainty, Chromatography, Uncertainty analysis, Chemistry, Environmental science, Mathematics

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