Systhesis and Charaterization of Mesoporous Molecular Sieve MCM-41 and TiO_2/MCM-41

Using industrial sodium silicate as silicate and surfactant C16H33(CH3)3NBr as structural template, the preparation of mesoporous molecular sieve MCM-41 was accomplished successfully by room temperature crystallization method, and and with tetrabutyltitanate as precursor, TiO2/MCM-41 loaded nanometer complex material was prepared by sol gel method and chemistry liquid deposit process. The samples were characterized by XRD、FT-IR, N2 adsorption/desorption at 77K and SEM. The results show that the end groups(Si-O-) of mesoporous molecular sieve MCM-41 react with Ti and the compound sample has characteristic peaks at 959 cm-1 due to Ti-O-Si formation; nano-TiO2 not only are well distributed the inner wall of mesoporous MCM-41, but also makes MCM-41 remain its ordered channel structure.