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Hydrothermal Synthesis and Crystal Structure of Coordination Compound [Cd(C_(10)H_7N_2O_2)_2·(H_2O)_4]n

Tian Yu-peng

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Abstract

A supermolecular compound [Cd(C10H7N2O2)2·(H2O)4]n was prepared under hydrothermal condition.The structure of the complex was determined by single crystal Xray diffraction analysis.The crystal belongs to monoclinic system with P2/c space group. The cell parameters are: a=1.234 9(5) nm,b=1.110 5(5) nm,c=0.801 4(5) nm,β=96.482(5)°,V=1.092 0(9) nm3,Z=2,Dc=1.699 g·cm-3,F(000)=564,wR=0.032.The crystal consists of units in which the Cd(II) ion is located in a slightly distorted octahedral center.Each units is connected by hydrogen bonds to form a threedimensional network structure.

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What this paper is about

A supermolecular compound [Cd(C10H7N2O2)2·(H2O)4]n was prepared under hydrothermal condition.The structure of the complex was determined by single crystal Xray diffraction analysis.The crystal belongs to monoclinic system with P2/c space group. The cell parameters are: a=1.234 9(5) nm,b=1.110 5(5) nm,c=0.801 4(5) nm,β=96.482(5)°,V=1.092 0(9) nm3,Z=2,Dc=1.699 g·cm-3,F(000)=564,wR=0.032.The crystal consists of units in which the Cd(II) ion is located in a slightly distorted octahedral center.Each units is connected by hydrogen bonds to form a threedimensional network structure.

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Available abstract

A supermolecular compound [Cd(C10H7N2O2)2·(H2O)4]n was prepared under hydrothermal condition.The structure of the complex was determined by single crystal Xray diffraction analysis.The crystal belongs to monoclinic system with P2/c space group. The cell parameters are: a=1.234 9(5) nm,b=1.110 5(5) nm,c=0.801 4(5) nm,β=96.482(5)°,V=1.092 0(9) nm3,Z=2,Dc=1.699 g·cm-3,F(000)=564,wR=0.032.The crystal consists of units in which the Cd(II) ion is located in a slightly distorted octahedral center.Each units is connected by hydrogen bonds to form a threedimensional network structure.

Key concepts: Monoclinic crystal system, Crystallography, Octahedron, Crystal structure, Hydrothermal circulation, Hydrothermal synthesis, Hydrogen bond, Chemistry

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Hydrothermal Synthesis and Crystal Structure of Coordination Compound [Cd(C_(10)H_7N_2O_2)_2·(H_2O)_4]n — Research Paper | ScholarLens